18色譜柱,以甲醇-0.4%磷酸水溶液為流動(dòng)相進(jìn)行梯度洗脫,體積流量 0.5 mL/min,柱溫 40 ℃。色譜條件(川芎):C18色譜柱,以甲醇-1%冰醋酸水溶液(32︰68)為流動(dòng)相,體積流量 1.0 mL/min,柱溫30 ℃。結(jié)果: 平均回收率分別為羥基紅花黃色素A 97.2%、RSD為2.3%(n=6);蘆丁99.6%、RSD為3.2%(n=6);川芎嗪100.9%、RSD為2.2%(n=6)阿魏酸98.6%、RSD為2.6%(n=6)。結(jié)論:本方法簡(jiǎn)便、快速、準(zhǔn)確,可作為血府逐瘀膠囊的原料藥材的質(zhì)量控制方法。;Objective: To establish the HPLC methods for the determination of hydroxysafflor yellow A and rutin in raw material and ligustrazine and ferulic acid in Ligusticum chuanxiong of Xuefuzhuyu Capsula and quantitative criteria for multi-component. Methods: The HPLC was applied with a C18 column for the determination of Carthamus tinctorius by gradient elution using methanol -0.4% phosphonic acid solution as the mobile phase. The flow rate was 0.5 mL/min and the temperature of column was 40?C. The HPLC was applied with a C18 column for the determination of L. chuanxiong using methanol -1.0% acetic acid solution (32︰68) as the mobile phase. The flow rate was 1.0 mL/min and the temperature of column was 30?C. Results: The average recovery rates were 97.2% ,99.6% ,100.9% , and 98.6%, RSD were 2.3%, 3.2%, 2.2%, and 2.6% for,hydroxysafflor yellow A and rutin, ligustrazine and ferulaic acid, respectively (n=6). Conclusion: The method is simple ,rapid, and accurate. It can be used for the quality control of Xuefuzhuyu Capsula."/>

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首頁(yè) > 過(guò)刊瀏覽>2010年第33卷第3期 >2010,33(3):206-209. DOI:10.7501/j.issn.0253-6376.[year].3.[sequence]
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血府逐瘀膠囊二次開(kāi)發(fā)中原料藥材質(zhì)量控制的研究

Research on quality control of the raw medicines in secondary development of Xuefuzhuyu Capsula

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