1H-NMR和13C-NMR)鑒定其結(jié)構(gòu)。結(jié)果 阿可拉定中2個(gè)主要雜質(zhì)分別為8-異戊烯基山柰酚和朝藿素B。結(jié)論 阿可拉定有關(guān)物質(zhì)的定量和定性研究可以為制定合理的雜質(zhì)限度提供依據(jù)。;Objective To purify and identify the main related substances of icraiin (IC-162). Methods Two main impurities were isolated from IC-162 with reverse phase silica gel and Sephedax LH-20. The structural characteristics of impurities were determined by spectral methods, such as LC-DAD, LC-MS, 1H-NMR, and 13C-NMR. Results The structures of two impurities were identified as 8-isopentenyl kaempferol and epimedokoreanin B. Conclusion With the quantitative and qualitative studies, the related impurities will be controlled in the reasonable limit."/>

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首頁 > 過刊瀏覽>2011年第34卷第2期 >2011,34(2):92-95. DOI:10.7501/j.issn.0253-6376.[year].2.[sequence]
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阿可拉定的有關(guān)物質(zhì)研究

Study on related substances of icraiin

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