目的 建立復(fù)方川芎滴丸的質(zhì)量標(biāo)準(zhǔn)。方法 采用薄層色譜法對(duì)復(fù)方中當(dāng)歸、川芎進(jìn)行了定性鑒別，采用高效液相色譜法對(duì)當(dāng)歸、川芎中阿魏酸進(jìn)行了定量測(cè)定。結(jié)果 薄層色譜分離度好；阿魏酸在0.001～0.100 mg/mL 與峰面積線性關(guān)系良好，平均回收率為102.06%，RSD 值為2.25%（n=6）。結(jié)論 所建立的方法準(zhǔn)確可靠，靈敏度高，專屬性強(qiáng)，可有效控制復(fù)方川芎滴丸的質(zhì)量。

Objective To establish the quality standard for Compound Chuanxiong Rhizoma Pills. Methods TLC method was performed to identify Angelica sinensis, Rhizoma Chuanxiong in Compound Rhizoma Chuanxiong Pills and HPLC was used to determine the content of ferulic acid in Angelica sinensis and Chuanxiong Rhizoma. Results TLC had good resolution and specificity. The ferulic acid showed a good liner relationship within the range of 0.001—0.1 mg/mL. The average recovery rate was 102.06% with RSD of 2.25%. Conclusion The method is accurate, specific, and could be used for the quality control of Compound Chuanxiong Rhizoma Pills.

軍隊(duì)醫(yī)療機(jī)構(gòu)制劑標(biāo)準(zhǔn)提高科研專項(xiàng)重點(diǎn)課題（13ZJZ02）