[關鍵詞]
[摘要]
目的 建立柴芩清熱膠囊的質量控制方法。方法 采用薄層色譜(TLC)法對組方中柴胡、連翹、訶子、大黃進行定性鑒別,采用高效液相色譜(HPLC)法測定黃芩苷。結果 薄層色譜清晰,分離良好,陰性無干擾。黃芩苷定量測定的平均回收率為98.39%,RSD為0.81%。結論 該方法簡便易行、靈敏準確、專屬性強,可用于柴芩清熱膠囊的質量控制。
[Key word]
[Abstract]
Objective To establish the quality control method of Chaiqin Qingre Capsules. Methods Bupleuri Radix, Forsythiae Fructus, Chebulae Fructus, and Rhei Radix et Rhizoma in the prescription were identified by thin layer chromatography (TLC);The baicalin content was quantitatively determined by high performance liquid chromatography (HPLC). Results The spots from the test solutions on the thin layer plate were clear and well separated without the negative interference. The average recovery rate of paeoniflorin was 98.39%, RSD was 0.81%. Conclusion This method is simple to operate, sensitive and accurate with strong specificity, which can be used to control the quality of Chaiqin Qingre Capsules.
[中圖分類號]
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