0.998,回收率在88.0%~107.3%,RSD值在0.1%~11.0%。結(jié)論 該方法簡便、快速、準確,可用于茯苓中藥材中17種元素的含量測定。;Objective The Chinese herbal medicine Poria as the research object, the determination of arsenic in Poria ICP-MS method (As), beryllium (Be), cadmium (Cd), cobalt (Co), copper (Cu), manganese (Mn), molybdenum (Mo), nickel (Ni), lead (Pb), antimony (Sb), selenium (Se), titanium (Ti), thallium (TI) and vanadium (V), chromium (Cr), zinc (Zn), mercury (Hg) content of 17 kinds of metal elements, and the content of metal elements in different places of the 11 batch of Poria was evaluated. It provides a scientific basis for quality control and clinical safety in the production of Chinese medicinal materials. Methods An Inductivety Coupled Plasma-Mass Spectrometry method with Microwave-Assisted Digestion was developed with Se, Y, In, In-1 and Bi as internal standard. Results For the determination of each element, the correlation coefficients were better than 0.998 0-0.999 9, the recovery values ranged from 88.0% to 107.3%, and the RSD values ranged from 0.1% to 11.0%.Conclusion The method is simple, rapid and accurate, and can be used for the determination of 17 elements in Chinese medicinal materials."/>

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首頁 > 過刊瀏覽>2019年第42卷第5期 >2019,42(5):890-894. DOI:10.7501/j.issn.1674-6376.2019.05.014
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電感耦合等離子體質(zhì)譜法測定茯苓中17種金屬元素

Determination of 17 elements in traditional Chinese medicine Poria by ICP-MS

發(fā)布日期:2019-05-31
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